Integrating The Gc, Msd, And Chemstation - HP 5973 Hardware Installation Manual

Mass selective detector
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Integrating the GC, MSD, and ChemStation

Materials needed:
MSD ChemStation software installation manual (G1701-90031)
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Be sure to select
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— Select
— When the pumpdown is complete, follow the instructions to set the GC/MSD
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— In the Diagnostics/Vacuum Control view, select
— Select
— Click
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— Click
— Click
— Click
— Do not run Autotune or the Air and Water Check at this time. The MSD must
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Select
Chemical Ionization
Diagnostics / Vacuum Control
Vacuum menu.
interface temperature to 280°C.
ATUNE.U
Diagnostics menu. Edit parameters as necessary.
from the MoreParams menu. Verify the MSD temperatures:
Temperatures
MS Source:
230°C
MS Quad:
150°C
to close the MS Zones dialog box.
OK
. Verify that there are peaks visible for all three masses.
Prof
. Click
.
Stop
MSOff
to close the Edit Parameters window.
OK
stabilize for at least 60 minutes.
Save Tune Values
from the File menu.
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for the CI MSD.
from the View menu. Select
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Edit MS Params
 Installation
from the
Pumpdown
from the
29

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