HP 5890 Series II Plus Reference Manual page 237

Test Sample Chromatograms
Test sample chromatograms
Figure 10-13.
Detector Type FPD
Temp 200 DEGREES C
Inlet Type PACKED OR PURGED
PACKED
Temp 200
Operating Mode
Purge Time On
Purge Time Off
Oven Temp Programmed (1 ramp)
Init Temp
Init Time
Ramp Rate
Fin Temp
Fin Time
Range 5
COLUMN:
Part No.
Dimensions
Sta Phase Methyl Silicone
IF
START
.07
1.73
TRIBUTYLPHOSPHATE
3.16
ZE
FPD Packed Column Inlet
HP 5890 Test Sample Operating
Conditions
DEGREES C
N/A
N/A min
N/A min
110 DEGREES C
0 min
___10
__170
____3
19095S•100
¿
5 M Length, 530 ID
Sulfer
Filter
DODECANETHIOL
2.11
FLOW RATES (FPD AIR MODE FLOWS)
Carrier (N2) 20 +/• 1
Hydrogen 75 +/• 2
Air 100 +/• 3
Makeup (N2)
Split Vent
Septum Purge
SAMPLE:
Type FPD Sample
¿
Inj Volume 1 l
Part No. 19395•60580
¿
COMPOSITION: 20 ng/
(20.0 ppm W/V) each of
1-dodecanethiol and
tributylphosphate in isooctane
START IF .07
Phospho-
.44
rus
Filter
DODECANETHIOL
2.10
2.46
ZE
ml/min
ml/min
ml/min
0 ml/min
N/A ml/min
1•2 ml/min
l
TRIBUTYLPHOS-
3.16
PHATE
237