HP 5890 Series II Plus Reference Manual page 238

Test Sample Chromatograms
Test sample chromatograms
Figure 10-14.
Detector Type FPD
Temp 200 DEGREES C
Inlet Type SPLIT ONLY OR
SPLIT/SPLITLESS
Temp 200
Operating Mode
Purge Time On
Purge Time Off
Oven Temp Programmed (1 ramp)
Init Temp
Init Time
Ramp Rate
Fin Temp
Fin Time
Range 5
COLUMN:
Part No.
Dimensions
Sta Phase Methyl Silicone
IF
START
.84
TRIBUTYLPHOS-
3.70
PHATE
ZE
FPD Split Mode Capillary Inlet
238
HP 5890 Test Sample Operating
Conditions
DEGREES C
SPLIT(PURGE ON)
0 min
0 min
110 DEGREES C
0 min
___10
_ 170
____3
19095Z•121
¿
5 M Length, 530 ID
.11
Sulfer
Filter
DODECANETHIOL
2.88
FLOW RATES (FPD AIR MODE FLOWS)
Carrier (N2) 20 +/• 1
Hydrogen 75 +/• 2
Air 100 +/• 3
Makeup (N2)
Split Vent 200 +/• 20
Septum Purge 5 +/• 1
SAMPLE:
Type FPD Sample
¿
Inj Volume 2 l
Part No. 19305•60580
¿
COMPOSITION: 20 ng/
(20.0 ppm W/V) each of
1-dodecanethiol and
tributylphosphate in isooctane
START
.71
DODECANETHIOL
2.88
ZE
ml/min
ml/min
ml/min
0 ml/min
ml/min
ml/min
l
.11
Phosphorus
Filter
3.70
TRIBUTYLPHOS-
PHATE